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dc.contributor.authorMeira, Manoel Messias Coutinho-
dc.contributor.authorLatteshttp://lattes.cnpq.br/1276479666609854por
dc.contributor.advisorPozza, Simone Andréa-
dc.contributor.advisorLatteshttp://lattes.cnpq.br/5530984461673946por
dc.contributor.advisor-co1Martinez, Diego Stéfani Teodoro-
dc.contributor.advisor-co1Latteshttp://lattes.cnpq.br/4898006494427762por
dc.contributor.advisor-co2Cristale, Joyce-
dc.contributor.advisor-co2Latteshttp://lattes.cnpq.br/6525387006649362por
dc.contributor.referees1Bettini, Jefferson-
dc.contributor.referees1Latteshttp://lattes.cnpq.br/3814895410100282por
dc.contributor.referees2Aguiar, Mônica Lopes-
dc.contributor.referees2Latteshttp://lattes.cnpq.br/0431688649128529por
dc.date.accessioned2024-05-09T16:34:53Z-
dc.date.issued2024por
dc.identifier.citationMEIRA, Manoel Messias Coutinho. Preparação e caracterização de filtros de TNT incorporados com Óxido de Grafeno para coleta de Material Particulado atmosférico. 2024. 91 p. Dissertação (Mestrado em Tecnologia) - Faculdade de Tecnologia, Universidade Estadual de Campinas, Limeira, 2024.por
dc.identifier.urihttps://deposita.ibict.br/handle/deposita/596-
dc.description.resumoA baixa qualidade do ar tem efeitos adversos para o clima, ecossistemas e para a saúde humana. O Material Particulado (MP) é um dos principais poluentes atmosféricos e representa uma séria preocupação para a saúde, sendo associada a doenças respiratórias e cardiovasculares, além de aumento das taxas de mortalidade. Entre os diferentes tamanhos de partículas, aquelas com menos de 100 nm de diâmetro (MP0,1) passam por transformações como modificações no tamanho, estrutura e composição química devido à sua alta área superficial e reatividade, sendo precursoras de partículas nocivas e persistentes. Entre as tecnologias de controle, os filtros e membranas contendo Óxido de Grafeno (GO) têm alta capacidade para capturar MP. Assim, objetiva-se com este trabalho, o desenvolvimento, caracterização e análise da filtração de particulado por filtros de Tecido Não Tecido de polipropileno (TNT-PP) incorporados com GO. Para tanto, a modificação de filtros meltblown comerciais com surfactante Pluronic F-127 e GO ocorreu por duas técnicas: spray e imersão, gerando um revestimento nanoestruturado sobre as microfibras. A caracterização dos flocos de GO foi realizada por Microscopia de Força Atômica (AFM). Enquanto as morfologias e composição dos filtros foram caracterizadas pela Microscopia Eletrônica de Varredura (MEV), perfilometria de contato, espectroscopia Raman, espectroscopia no infravermelho por transformada de Fourier (FT-IR) e tensiometria para ensaio de ângulo de contato. As imagens MEV demonstraram a conformação das fibras, bem como a evolução da formação do filme a partir da deposição de camadas de spray de GO. Os filtros TNT-PP/GO também foram avaliados quanto à captura do particulado por um Analisador de Partículas por Mobilidade Elétrica (SMPS). Nesse contexto, a eficiência de filtração do MP0,1 é maior no meio filtrante funcionalizado (80,4%) em comparação ao filtro sem cobertura (66,2%) devido à presença de grupos funcionais oxigenados do GO. Além da manutenção da baixa queda de pressão (18,6 Pa) e fator de qualidade ~0,086 Pa-1 para a vazão do gás de 1,5 L/min. Assim, o protocolo de incorporação por spray revelou-se eficaz no melhoramento do meio filtrante, apresentando-se como uma estratégia viável e promissora para o desenvolvimento de novos materiais.por
dc.description.abstractPoor air quality has adverse effects on climate, ecosystems, and human health. Airborne particulate matter (PM) is one of the main atmospheric pollutants, and poses a serious threat to health, being associated with respiratory and cardiovascular diseases, in addition to an increased rate of mortality. Among the different particle sizes, those with less than 100 nm (PM0.1) undergo transformations like size modifications, structure, and chemical composition due to their high surface area and reactivity, being precursors of harmful and persistent particles. Among the control technologies, filters and membranes containing Graphene Oxide (GO) have a high capacity to capture PM. Thus, this work aims at the fabrication, characterization, and analysis of the filtration of particulate through polypropylene nonwoven fabric (NWF-PP) filters incorporated with GO. Therefore, commercial meltblown filters modification with the surfactant Pluronic F-127 and GO occurred by two techniques: spraying and immersion, generating a nanostructured coating over the microfibers. The GO flakes characterization was performed through atomic force microscopy (AFM). While the filters morphologies and composition were characterized by scanning electron microscopy (SEM), contact profilometry, Raman spectrometry, Fourier-transform infrared spectroscopy (FT-IR), and tensiometry for contact angle measurement. SEM images show the fibers conformation, as well as the evolution of the film formation from GO spray layers deposition. The NWF-PP filters also had their particle capture efficiency evaluated by a scanning mobility particle sizer (SMPS). In this context, the filtration efficiency of PM0.1 is higher in the functionalized filter medium (80.4%) in comparison with the uncovered filter (66.2%) due to the presence of oxygen-containing functional groups. In addition to low pressure drop (18.6 Pa) and quality factor ~0.086 Pa-1 for gas flow rate at 1.5 L/min. Thus, the incorporation protocol turned out to be efficient in the enhancement of the filter medium, emerging as a viable and promising strategy for new materials development.eng
dc.description.provenanceSubmitted by Manoel Meira (manoelcmeira@gmail.com) on 2024-05-07T01:43:58Z No. of bitstreams: 1 Defesa - Mestrado - Final.pdf: 4189321 bytes, checksum: 81508421b7183b88937abbf87df44787 (MD5)eng
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dc.description.sponsorshipCoordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)por
dc.formatapplication/pdf*
dc.languageporpor
dc.publisherUniversidade Estadual de Campinas (UNICAMP)por
dc.publisher.departmentFaculdade de Tecnologia (FT)por
dc.publisher.countryBrasilpor
dc.publisher.programPrograma de Pós-graduação em Tecnologia (PPGT)por
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dc.rightsopenAccesspor
dc.subjectadsorçãopor
dc.subjectfiltros de arpor
dc.subjectmaterial particuladopor
dc.subjectpolipropilenopor
dc.subjectadsorptioneng
dc.subjectair filterseng
dc.subjectparticulate mattereng
dc.subjectpolypropyleneeng
dc.subject.cnpqControle da poluiçãopor
dc.subject.cnpqEngenhariaspor
dc.subject.cnpqQuímicapor
dc.titlePreparação e caracterização de filtros de TNT incorporados com Óxido de Grafeno para coleta de Material Particulado atmosféricopor
dc.title.alternativePreparation and characterization of Nonwoven Fabric Filters incorporated with Graphene Oxide for atmospheric Particulate Matter removaleng
dc.typemastherThesispor
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