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Synthesis and Characterization of Two Novel Naphthalenediimide/ Zinc Phosphonate Crystalline Materials Precipitated from Different Solvents
| Página final: | 1756 |
| Página inicial: | 1748 |
| Volume: | 9 |
| Autor: | Poly-Anna Vera Melo, Barbra |
| Autor: | Fernando Gregório Junior, Denis |
| Autor: | Troilo de Oliveira, Matheus |
| Autor: | de Jesus Trindade, Fabiane |
| Autor: | van de Streek, Jacco |
| Autor: | Furlan Ferreira, Fabio |
| Autor: | Brochsztain, Sergio |
| Data de Acesso: | 2024-11-11T19:20:57Z |
| Ano de publicação: | 2024 |
| Abstract: | Hybrid naphthalenediimide/zinc phosphonate materials (NDI/Zn) were prepared by mixing solutions of N,N′-bis(2- phosphonoethyl)-1,4,5,8-naphthalenediimide (PNDI) and zinc nitrate, resulting in the precipitation of the desired compounds. Samples precipitated from water and N,N-dimethylformamide (DMF) were produced. The obtained samples had the expected elemental composition, and the presence of naphthalenediimides (NDI) was ascertained by infrared and UV−visible spectroscopy. All the samples were crystalline, according to powder X-ray diffraction. Nitrogen adsorption isotherms showed the presence of porosity in the NDI/Zn samples. Mesopores with a diameter = 4.1mm were present in the sample from DMF, with total pore volume reaching 0.13 cm3/g. |
| Proveniência: | Submitted by Sergio Brochsztain (sergio.brochsztain@ufabc.edu.br) on 2024-10-29T23:53:00Z No. of bitstreams: 1 (49) ACS Omega 2024.pdf: 7180988 bytes, checksum: cbb9e6aef7ca1e4ff153c3034d800f06 (MD5) |
| Proveniência: | Approved for entry into archive by Cássio Morais (cassiomorais@ibict.br) on 2024-11-11T19:20:57Z (GMT) No. of bitstreams: 1 (49) ACS Omega 2024.pdf: 7180988 bytes, checksum: cbb9e6aef7ca1e4ff153c3034d800f06 (MD5) |
| Proveniência: | Made available in DSpace on 2024-11-11T19:20:57Z (GMT). No. of bitstreams: 1 (49) ACS Omega 2024.pdf: 7180988 bytes, checksum: cbb9e6aef7ca1e4ff153c3034d800f06 (MD5) Previous issue date: 2024 |
| Região: | Sudeste |
| Resumo: | Hybrid naphthalenediimide/zinc phosphonate materials (NDI/Zn) were prepared by mixing solutions of N,N′-bis(2- phosphonoethyl)-1,4,5,8-naphthalenediimide (PNDI) and zinc nitrate, resulting in the precipitation of the desired compounds. Samples precipitated from water and N,N-dimethylformamide (DMF) were produced. The obtained samples had the expected elemental composition, and the presence of naphthalenediimides (NDI) was ascertained by infrared and UV−visible spectroscopy. All the samples were crystalline, according to powder X-ray diffraction. Nitrogen adsorption isotherms showed the presence of porosity in the NDI/Zn samples. Mesopores with a diameter = 4.1 nm were present in the sample from DMF, with total pore volume reaching 0.13 cm3/g. |
| Agência de financiamento: | Fundação de Amparo à Pesquisa do Estado de São Paulo |
| Formato: | application/pdf |
| URI: | https://deposita.ibict.br/handle/deposita/690 |
| Idioma: | eng |
| Instituição: | Universidade Federal do ABC |
| País: | Estados unidos |
| Título do periódico: | ACS Omega |
| Tipo de acesso: | openAccess |
| Palavra Chave: | Metal Phosphonates |
| Palavra Chave: | Zinc Phosphonate |
| Palavra Chave: | Naphthalenediimides |
| Palavra Chave: | Mesoporous Materials |
| Área de conhecimento CNPq: | Química |
| Título: | Synthesis and Characterization of Two Novel Naphthalenediimide/ Zinc Phosphonate Crystalline Materials Precipitated from Different Solvents |
| Tipo: | Artigo |