Synthesis and Characterization of Two Novel Naphthalenediimide/ Zinc Phosphonate Crystalline Materials Precipitated from Different Solvents
| Página final | 1756 | por |
| Página inicial | 1748 | por |
| Volume | 9 | por |
| Autor | Poly-Anna Vera Melo, Barbra | |
| Autor | Fernando Gregório Junior, Denis | |
| Autor | Troilo de Oliveira, Matheus | |
| Autor | de Jesus Trindade, Fabiane | |
| Autor | van de Streek, Jacco | |
| Autor | Furlan Ferreira, Fabio | |
| Autor | Brochsztain, Sergio | |
| Data de Acesso | 2024-11-11T19:20:57Z | |
| Ano de publicação | 2024 | por |
| Abstract | Hybrid naphthalenediimide/zinc phosphonate materials (NDI/Zn) were prepared by mixing solutions of N,N′-bis(2- phosphonoethyl)-1,4,5,8-naphthalenediimide (PNDI) and zinc nitrate, resulting in the precipitation of the desired compounds. Samples precipitated from water and N,N-dimethylformamide (DMF) were produced. The obtained samples had the expected elemental composition, and the presence of naphthalenediimides (NDI) was ascertained by infrared and UV−visible spectroscopy. All the samples were crystalline, according to powder X-ray diffraction. Nitrogen adsorption isotherms showed the presence of porosity in the NDI/Zn samples. Mesopores with a diameter = 4.1mm were present in the sample from DMF, with total pore volume reaching 0.13 cm3/g. | eng |
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| Região | Sudeste | por |
| Resumo | Hybrid naphthalenediimide/zinc phosphonate materials (NDI/Zn) were prepared by mixing solutions of N,N′-bis(2- phosphonoethyl)-1,4,5,8-naphthalenediimide (PNDI) and zinc nitrate, resulting in the precipitation of the desired compounds. Samples precipitated from water and N,N-dimethylformamide (DMF) were produced. The obtained samples had the expected elemental composition, and the presence of naphthalenediimides (NDI) was ascertained by infrared and UV−visible spectroscopy. All the samples were crystalline, according to powder X-ray diffraction. Nitrogen adsorption isotherms showed the presence of porosity in the NDI/Zn samples. Mesopores with a diameter = 4.1 nm were present in the sample from DMF, with total pore volume reaching 0.13 cm3/g. | por |
| Agência de financiamento | Fundação de Amparo à Pesquisa do Estado de São Paulo | por |
| Formato | application/pdf | * |
| URI | https://deposita.ibict.br/handle/deposita/690 | |
| Idioma | eng | por |
| Instituição | Universidade Federal do ABC | por |
| País | Estados unidos | por |
| Título do periódico | ACS Omega | por |
| Tipo de acesso | openAccess | por |
| Palavra Chave | Metal Phosphonates | eng |
| Palavra Chave | Zinc Phosphonate | eng |
| Palavra Chave | Naphthalenediimides | eng |
| Palavra Chave | Mesoporous Materials | eng |
| Área de conhecimento CNPq | Química | por |
| Título | Synthesis and Characterization of Two Novel Naphthalenediimide/ Zinc Phosphonate Crystalline Materials Precipitated from Different Solvents | por |
| Tipo | Artigo | por |